Page 78 - Plastics News July 2025
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PRODUCT NEWS








          to develop new hybrid formulations by incorpo-        system. This setup allowed the team to validate
          rating CNTs into the micronized amide resin. The      rheological findings from creep tests, oscillatory
          addition of CNTs significantly increased the yield    sweeps, and flow curves.
          stress—reaching 1400 Pa with 0.5 wt% CNT—
          and improved sag resistance. This enables the
          resin to bridge spans up to 20 times the noz-
          zle diameter. However, extrudability decreased,
          making the material too viscous for fine nozzles
          (e.g., 18 gauge).

          Despite this issue, the  formulation with 15 wt%
          micronized amide and 0.5 wt% CNT proved to
          be the most effective combination.


                                                                Formulation Innovations for Superior EDAM Per-
                                                                formance


                                                                Overall, this study demonstrates the benefits of
                                                                combining additives to achieve superior resin
                                                                formulations. By mixing micronized amide with
          Connecting Lab Rheometer Data to Real-World           CNTs, the resin exhibited increased yield stress
          Print Performance                                     and enhanced sag resistance. This significantly
                                                                improved bridging performance. In the best case,
          Beyond developing a new resin formulation for         the resin showed excellent sag resistance. The
          EDAM, one of the study’s most significant break-      total sag measured less than one nozzle height
          throughs was the connection between laborato-         over a span of 20 times the nozzle diameter.
          ry results and real-world printing performance.
          The  research  team  conducted  rheology  and         Researchers noted that further studies are
          bridging tests to directly link material behavior     needed to reduce the shear thinning exponent
          to actual print outcomes.                             and increase the elastic modulus at high shear
                                                                rates. Despite this, the results represent a sig-
          To physically evaluate span bridging, they built a    nificant advancement for EDAM of sparse infill
          custom testing apparatus. While lab-scale meas-       structures.  With  these  new  formulations,  such
          urements provided controlled, quantifiable data,      structures could become not only lightweight
          the real-world simulation demonstrated wheth-         and cost-effective but also exhibit improved
          er those rheological properties translated into       mechanical properties. This opens the door to
          practical printing success.                           broader applications across various industries.


          The bridging fixture included a syringe pump                               Source – PLASTICS ENGINEERING
          with 18-gauge nozzles, a linear slide table with
          an aluminum bridging platform, and a camera

             78   PLASTICS NEWS                                                                         July 2025
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